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Abstract. To determine which structural features may favor electron transfer in biological systems, cyclic voltammetric studies were carried out on conjugated aliphatic ketone, oxime, and imine species at pH levels 2 through 7 in most cases. The nature of the conjugated substituents strongly influenced the reduction potentials. The dione samples were most easily reduced, followed by the diimine and then the mono- and di-oxime analogs. The reduction potentials for all compounds were pH-dependent, with the most favorable potentials occurring at the lower pH values. The possible roles of protonation, hydrogen bonding, the captodative effect, and other aspects were considered. The favorable reduction potentials of the compounds exhibiting bioactivity suggest that in vivo electron transfer and oxidative stress may be involved in various types of biological processes. Keywords: Cyclic voltammetry; diones; diimines; dioximes; bioactive; electron transfer; oxidative stress. Resumen. Para determinar las caractersticas estructurales que pueden favorecer la transferencia electrnica en sistemas biolgicos, se llevaron a cabo estudios de voltametra cclica en cetonas conjugadas, oximas e iminas a pH de naturaleza de los substituyentes conjugados tienen notable influencia en los potenciales de reduccin. Las dionas se reducen ms fcilmente, seguido por las diiminas y los anlogos mono- y di- oximas. Los potenciales de reduccin de todos los compuestos son dependientes del pH, y las potencias ms favorables se encuentran a pH bajos. Los posibles efectos de protonacin, formacin de puente de hidrgeno, efecto captodativo, y otros aspectos, tambin fueron considerados. Los potenciales de reduccin favorables de los compuestos que muestran actividades biolgicas sugieren que la transferencia electrnica in vivo y el estrs oxidativo pueden estar involucrados en varios tipos de procesos biolgicos. Palabras clave: Voltametra cclica, dionas, diiminas, dioximas, bioactividad, transferencia electrnica, estrs oxidativo.
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Received August 9, 2003. Accepted for publication May 5, 2004. Authors' addresses: Krishna Pandey, Prabhat K. Sinha, Vidyan N. Ravidas, Nawin Kumar, Neena Verma, Chandra S. Lal, Sanjeev Bimal, and Sujit K. Bhattacharya, Rajendra Memorial Research Institute of Medical Sciences, Agam Kuan, PO Gulzarbagh, Patna 800007, Bihar, India. Dipika Sur, National Institute of Cholera and Enteric Diseases, P-33, CIT Road, Scheme XM, Beliaghata, Kolkata 700010, India. Reprint requests: Sujit K. Bhattacharya, Rajendra Memorial Research Institute of Medical Sciences, Agam Kuan, PO Gulzarbagh, Patna 800007, Bihar, India, Telephone: 91-33-2-350-1176, Fax: 91-332-350-5066 or 91-33-2-353-2524, E-mail: bsandip cal3.vsnl .in or bsujit vsnl and rifampin and seroquel, for instance, drug more serlquel use.
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